Synthesis, characterization and degradation activity of Methyl orange Azo dye using synthesized CuO/α-Fe2O3 nanocomposite

نویسندگان

  • Mansour Jahangiri Faculty of Chemical, Petroleum and Gas Engineering, Semnan University, Semnan, Iran
چکیده مقاله:

This study investigated the photo-degradation of methyl orange (MO) as a type of azo dye using a CuO/α-Fe2O3 nanocomposite. A CuO/α-Fe2O3 powder with a crystalline size in the range of 27-49 nm was successfully prepared using simple co-precipitation along with a sonication method. The characterization of the synthesized sample was done via XRD, FE-SEM, EDS, FTIR and DRS analyses. The Tauc equation revealed that the band gap of the nano composite in the direct mood was 2.05 ev, which is in the visible light range. The effect of operating factors containing dye concentration, photocatalyst dosage and pH on dye degradation efficiency was measured. Response Surface Method (RSM) was employed to specify the parameter effects. The photocatalytic activity of the CuO/α-Fe2O3 nanocomposite was evaluated by degradation of MO under visible light irradiation. The results showed that the pH value played a very effective role in the dye degradation process efficiency. Also, the photocatalytic degradation of MO obtained was equal to 88.47% in the optimal values. 

برای دانلود باید عضویت طلایی داشته باشید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Microwave-assisted Synthesis of MgFe2O4-ZnO Nanocomposite and Its Photo-catalyst Investigation in Methyl Orange Degradation

In this work firstly MgFe2O4 nanoparticles were synthesized via a microwave-assisted method. The product was calcinated at 900 ºC for 2h. At the second step zinc oxide shell was synthesized on the ferrite under ultrasonic waves. Properties of the product were examined by X-ray diffraction pattern (XRD), scanning electron microscope (SEM) and Fourier transform infrared (FT-IR) spectroscopy. Vibr...

متن کامل

Synthesis, characterization and sonophotocatalytic degradation of an azo dye on Europium doped cadmium selenide nanoparticles

In this study, Eu-doped CdSe nanoparticles with variable Eu3+ content were synthesized by a simple sonochemical method. Eu3+ substitution into the structure of CdSe resulted in a material with new physical properties, composition and morphology. The synthesized nanoparticles were characterized by powder X-ray diffraction (XRD), scanning electron microscopy (SEM), X-ray photoelectron spectroscop...

متن کامل

Photocatalyst Ag@N/TiO2 Nanoparticles: Fabrication, Characterization, and Investigation of the Effect of Coating on Methyl Orange Dye Degradation

In this research, N-doped TiO2 (N/TiO2) nanoparticles have been synthesized by a sol-gel method. N/TiO2 nanoparticle has been coated with Ag metal by photochemical method. Triethylamine, N(CH3CH2)3, have been used as precursors of Nitrogen, titanium tetraiso-propoxide (TTIP), Ti[OCH(CH3)2]4, used as precursors of titanium and Ag(NO3)2 used as precursors of Silver in synthesis of these nanoparti...

متن کامل

microwave-assisted synthesis of mgfe2o4-zno nanocomposite and its photo-catalyst investigation in methyl orange degradation

in this work firstly mgfe2o4 nanoparticles were synthesized via a microwave-assisted method. the product was calcinated at 900 ºc for 2h. at the second step zinc oxide shell was synthesized on the ferrite under ultrasonic waves. properties of the product were examined by x-ray diffraction pattern (xrd), scanning electron microscope (sem) and fourier transform infrared (ft-ir) spectroscopy. vibr...

متن کامل

منابع من

با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

ذخیره در منابع من قبلا به منابع من ذحیره شده

{@ msg_add @}


عنوان ژورنال

دوره 2  شماره 3

صفحات  143- 151

تاریخ انتشار 2017-04-22

با دنبال کردن یک ژورنال هنگامی که شماره جدید این ژورنال منتشر می شود به شما از طریق ایمیل اطلاع داده می شود.

میزبانی شده توسط پلتفرم ابری doprax.com

copyright © 2015-2023